Author: Zhang, Ze; Peng, Zhi-Wei; Hao, Ming-Feng; Gao, Jian-Gang
Description: Under mechanochemical milling conditions, Diels-Alder cycloaddition of cyclopentadiene with maleic anhydride and maleimide derivatives proceeded very smoothly, affording endo-norbornenes exclusively in quantitative yield. All the transformations were accomplished at room temperature without using any catalyst or organic solvent, thus the workup and purification procedure is very simple. Control experiments on traditional and other tentative conditions were also investigated.
Subject headings: Norbornenes; Mechanochemical milling; Solvent-free; Cyclopentadiene; Diels-Alder reaction
Publication year: 2010
Journal or book title: Synlett
Issue: 19
Pages: 2895-2898
Find the full text: https://www.thieme-connect.com/products/ejournals/abstract/10.1055/s-0030-1259030
Find more like this one (cited by): https://scholar.google.com/scholar?cites=11104987599590425377&as_sdt=5,26&sciodt=0,26&hl=en
Serial number: 3345